分析化学作为科学研究的 “眼睛”，始终扎根于多学科交叉的沃土。从医药研发中痕量杂质的精准捕捉，到环境监测里超微量污染物的追踪，再到新材料表征中分子结构的解析，其技术突破直接推动着生命科学、生态保护与工业革新的边界。

本期刊•见为诸位介绍一本聚焦分析化学及相关测量科学领域期刊 Critical Reviews in Analytical Chemistry。除了对关键指标进行详尽解读外，还将向您推荐刊内近三年高被引文章，以及近一年高阅读量文章：

• 影响采用超声波辅助提取结合深共晶溶剂从天然资源中提取（聚）酚类物质的因素

• 基于钼的电化学传感器在乳腺癌生物标志物检测中的应用：进展与挑战

• 威胁因子早期检测：生物免疫传感器的综述及其发展前景

Print ISSN: 1040-8347 Online ISSN: 1547-6510

Critical Reviews in Analytical Chemistry始终致力于为专家学者和学生提供可靠的高水平学术资源，聚焦分析化学与测量科学领域的重要主题，发表深度、富有洞见的学术综述，旨在阐释科学本质、结合最新进展客观评估学科现状，并展望未来发展方向。该刊致力于以跨学科方式联结不同基础研究组成部分，并保持应用与基础研究之间的平衡，关注的主题包括但不仅限于：化学分析、仪器分析、化学计量学、分析生物化学、药物分析、法医学、环境科学、应用物理学。

该期刊已被SCIE、Medline、Scopus、EBSCOhost等核心数据库收录。

影响因子

根据JCR显示，Critical Reviews in Analytical Chemistry 在分析化学排名 22/111

CiteScore

根据Scopus显示, Critical Reviews in Analytical Chemistry

2024年CiteScore为 12.5

在化学：分析化学领域排名 11/160

中国科学院文献情报中心期刊分区表

根据2025年3月20日发布的中国科学院文献情报中心期刊分区表显示：

大类及分区：化学3区

小类及分区：分析化学3区

审稿周期

从提交稿件到获取初审意见，平均需要21天

从提交稿件到获取首个同行评审后的决定，平均需要35天

稿件一旦接受后，在线出版平均需要17天

Critical Reviews in Analytical Chemistry期刊的主编现由美国犹他州立大学（Utah State University, USA）的Stephen E. Bialkowski教授担任，副主编由来自巴西戈亚斯联邦大学（Federal University of Goiás, Brazil）的Ana Carolina Kogawa担任，编辑团队汇集来自美国、西班牙、中国等地的行业翘楚。

主编

Stephen E. Bialkowski

美国犹他州立大学（Utah State University, USA）化学与生物化学系荣誉教授，作为分析化学领域的资深学者，他的研究兴趣包括分析化学仪器、分析方法开发、液相色谱等。

中国编委

胥传来

中国江南大学教授、博士生导师，主要研究领域为生物界面与生物检测。

根据JCR显示，近三年在 Critical Reviews in Analytical Chemistry 发文的国家/地区中，发文较为活跃的有：

中国

印度

沙特阿拉伯

近三年，在 Critical Reviews in Analytical Chemistry 发文的全球高校和科研机构中，发文较为活跃的有：

中国医科大学

土耳其安卡拉大学

埃及知识库（EKB）

影响采用超声波辅助提取结合深共晶溶剂从天然资源中提取（聚）酚类物质的因素

作者：Shahida Anusha Siddiqui et al.

文章摘要：

Replacing conventional solvents with deep eutectic solvents (DES) has shown promising effects on the extraction yield of (poly)phenols. DES can be combined with ultrasound-assisted extraction (UAE) to further increase the extraction efficiency of (poly)phenols from natural resources compared to conventional methods. This review discusses the factors associated with DES (composition, solvent-to-sample ratio, extraction duration, and temperature) and UAE (ultrasound frequency, power, intensity, and duty cycle) methods that influence the extraction of (poly)phenols and informs future improvements required in the optimization of the extraction process. For the optimum (poly)phenol extraction from natural resources, the following parameters shall be considered: ultrasound frequency should be in the range of 20–50 kHz, ultrasound intensity in the range of 60–120 W/cm2, ultrasound duty cycle in the range of 40–80%, ultrasound duration for 10–30 minutes, and ultrasound temperature for 25–50 °C. Among the reported DES systems, choline chloride with glycerol or lactic acid, with a solvent-to-sample mass ratio of 10–30:1 shown to be effective. The solvent composition and solvent-to-sample mass ratio should be selected according to the target compound and the source material. However, the high viscosity of DES is among the major limitations. Optimizing these factors can help to increase the yield of extracted (poly)phenols and their applications.

Figure 2. Ultrasound-assisted extraction with deep eutectic solvents (DES-UAE) process and extraction mechanism of (poly)phenols.

基于钼的电化学传感器在乳腺癌生物标志物检测中的应用：进展与挑战

作者：Aliya Sarsenbayeva et al.

文章摘要：

Breast cancer, which is considered the most common type of cancer among women worldwide, is estimated to reach 4.4 million cases in 2070. Early diagnosis has become very important to prevent this expected increase. Various traditional methods, such as mammography, biopsy, enzyme immunoassay (EI), liquid biopsy, immunohistochemistry (IGH), fluorescence in situ hybridization (FISH) are used to diagnose breast cancer, but the fact that these methods are very expensive, have low sensitivity, and cause mutations in tissues due to X-rays has led researchers to discover faster, more cost-effective, and easily detectable methods. In particular, increased levels of new blood-based biomarkers in the circulation can be detected sensitively and selectively by electrochemical methods to facilitate early disease screening and rapid diagnosis. This comprehensive review focuses on the prevalence and pathology of breast cancer, clinical diagnosis of breast cancer, and electrochemical sensors of molybdenum-based compounds for the detection of various breast cancer biomarkers in recent years. Electrochemical analysis studies carried out in the field in recent years are compiled and are considered as aptamer-based, nucleotide-based, and immunosensors. The chemical properties of molybdenum compounds are discussed, and the modifications of these compounds to the electrode surface are discussed under 4 headings: drop casting, electrodeposition, atomic layer deposition, and electrophoretic deposition.

Figure 1. Schematic representation of drop casting from electrode surface modification approaches.

威胁因子早期检测：生物免疫传感器的综述及其发展前景

作者：Karolina Morawska et al.

【查阅全文内容】

文章摘要：

Early detection of biological threat agents plays a crucial role in public health protection, food safety, and environmental monitoring. Bioimmunosensors, utilizing specific antigen-antibody interactions, represent a promising technology in these applications due to their high sensitivity and specificity. This review explores the current state of knowledge regarding bioimmunosensors, highlighting recent technological innovations, such as integration with nanotechnology, microfluidic techniques, and the development of novel detection platforms based on optical and electrochemical biosensors. Key challenges in their development, including the stability of biological detection elements, cost reduction, and the scalability of technology for real-world applications, are also discussed. The analysis of future application prospects points to the growing potential of bioimmunosensors in areas such as medical diagnostics, pathogen detection in the environment, food quality control, and bioterrorism defense. Increased integration of bioimmunosensors with the Internet of Things (IoT) systems and the development of portable analytical devices may revolutionize the approach to monitoring and rapid response to biological threats in the coming years.

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