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Appl. Phys. Lett. bulk-metallic glass

已有 7303 次阅读 2007-12-27 22:03 |个人分类:非晶前沿

Characterization of fatigue-induced free volume changes in a bulk metallic glass using positron annihilation spectroscopy

Appl. Phys. Lett. 91, 261908 (2007) (3 pages)

Published 26 December 2007

R. S. Vallery, M. Liu, and D. W. Gidley
Department of Physics, University of Michigan, Randall Laboratory, Ann Arbor, Michigan 48109, USA

M. E. Launey and J. J. Kruzic

Materials Science, School of Mechanical, Industrial, and Manufacturing Engineering, Oregon State University, Corvallis, Oregon 97331, USA

Depth-profiled Doppler broadening spectroscopy of positron annihilation on the cyclic fatigue-induced fracture surfaces of three amorphous Zr44Ti11Ni10Cu10Be25 metallic glass specimens reveals the presence of a 30–50  nm layer of increased free volume that is generated by the propagating fatigue crack tip. The presence and character of this fatigue transformation zone is independent of the initial amount of bulk free volume, which was varied by structural relaxation via annealing, and the voids generated in the zone by intense cyclic deformation are distinct from those typical of the bulk. ©2007 American Institute of Physics


Fe–Zr–Nd–Y–B permanent magnet derived from crystallization of bulk amorphous alloy

Appl. Phys. Lett. 91, 252501 (2007) (3 pages)

Published 18 December 2007


Institute of Materials Science, Shanghai University, Shanghai 200072, People's Republic of China

The microstructure and magnetic properties of Nd2Fe14B/(Fe3B,alpha-Fe) nanocomposite magnet derived form crystallization of bulk amorphous Fe68Zr2Y4B21Nd5 alloy, which was prepared by copper mold casting, have been investigated. The obtaining maximum values of Ms, Mr, iHc, and (BH)max annealed at 963  K for Fe68Zr2Nd5Y4B21 alloy are 86  A  m2/kg, 49  A  m2/kg, 380  kA/m, and 43  kJ/m3, respectively. deltaM plot, high resolution transmission electron microscopy observation, and three-dimensional atom probe technique clarified that the hard magnetic behavior is due to the exchange coupling between soft and hard magnetic nanophases. ©2007 American Institute of Physics

About this Journal

Spatiotemporally inhomogeneous plastic flow of a bulk-metallic glass

W.H. Jianga, Corresponding Author Contact Information, E-mail The Corresponding Author, G.J. Fana, F.X. Liua, G.Y. Wanga, H. Chooa, b and P.K. Liawa

Abstract

With geometrically-constrained specimens, the spatiotemporally inhomogeneous deformation of a Zr-based bulk-metallic glass in uniaxial, quasistatic, compression was investigated. Decreasing the height/width ratio of specimens from 2 to 0.5 significantly increases the plastic strain from 2% to about 80%. Using an infrared camera, we first observe in situ dynamic shear-banding operations during compression at various strain rates. The shear banding is highly dependent on strain rates, either intermittent at the lower strain rate or successive at the higher strain rate. Scanning electron microscopy observations show the spatiality of the rate-dependent shear banding. The serrated plastic flow is a result of the shear-banding operations. At the lower strain rate, more simultaneous shear-banding operations result in more obvious serrations, while at the higher strain rate, fewer simultaneous shear-banding operations cause less obvious serrations.


Keywords: Bulk amorphous materials; A. Ductility; B. Glass material; C. Nondestructive evaluation; D. Metallic material


aDepartment of Materials Science and Engineering, The University of Tennessee, Knoxville, TN 37996, United States
bMaterials Science and Technology Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831, United States
Received 28 May 2006;  revised 9 January 2007.  Available online 8 February 2007.



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